How to make LSD

MANUFACTURE OF LSD

Materials:

1. Ergotamine tartrate

2. Hydrazine hydrate

3. Hydrazide

4. Hydrochloric Acid

5. Sodium Nitrite

6. Sodium Bicarbonate

7. Diethylamine

8. Ether

9. Flasks

10. Filter paper

11. Heating mantle

12. 2 liter three-necked round bottom flask

Time: Approximately 36 hours.

Process:

STEP 1: In a 2 liter three-necked round bottom flask
add to 2 grams of ergotamine tartrate about 1/2 gram
of hydrazine hydrate. Exercise caution when adding
the hydrazine hydrate because it is very poisonous,
particularly to the eyes.

STEP 2: Place a condensing column on one neck of the
flask. Place a stirring device in the center neck and
place a separatory funnel in the thick neck. (Note:
hydrazide hydrate may be added through a separatory
funnel although it is not necessary.)

STEP 3: Place the flask on a heating mantle and simmer
the solution for 2-3 hours while stirring occasionally.

STEP 4: Remove condensing column from flask and continue
to cook for 10-15 minutes or until the original solution
is reduced by half.

STEP 5: After solution has cooled, pour the solution
through filter paper and collect the crystals that
formed. Wash the crystals in a small amount of
absolute alcohol.



STEP 6: Dissolve the crystals in about 30cc of diluted
hydrochloric acid. (Note: diluted hydrochloric acid is
mixed at a rate of 1 part acid to 10 or 15 parts water.)

STEP 7: To the hydrochloric acid solution add about
15cc of a solution of sodium nitrite diluted in water.
(Note: one part sodium nitrite to 10 or 15 parts
water.) Let this solution stand for about 30 minutes.

STEP 8: To this solution add about one teaspoonful of
sodium bicarbonate (baking soda) to make the solution
basic.

STEP 9: Place this solution in a separatory funnel and
add to it an equal quantity of ether. Shake this
solution gently for about 5 minutes.

STEP 10: Separate the ether solution from the
separatory funnel and keep the ether solution. The
remainder may be discarded.

STEP 11: Cool the ether solution to 0 degrees Celsius
and to the solution add a solution of about .5 gram
of diethylamine mixed with ether.

STEP 12: Maintain the solution at 0 degrees Celsius for
24 hours, stirring it occasionally (perhaps 4 hour
intervals.)

STEP 13: Remove the solution from the ice bath and
allow it to stand at room temperature for about 2
hours, or until it evaporates. The remaining crystals
will be crude LSD.

STEP 11: Cool the ether solution to 0 degrees Celsius
and to the solution add a solution of about .5 gram
of diethylamine mixed with ether.

STEP 12: Maintain the solution at 0 degrees Celsius for
24 hours, stirring it occasionally (perhaps 4 hour
intervals.)

STEP 13: Remove the solution from the ice bath and
allow it to stand at room temperature for about 2
hours, or until it evaporates. The remaining crystals
will be crude LSD.

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